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Surface chemical conversion of 3-glycidoxypropyldimethylethoxysilane on hydroxylated silicon surface: FT-IR, contact angle and ellipsometry analysis

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Date

2012

Author

Demirci, Serkan
Kinali-Demirci, Selin
Caykara, Tuncer

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Abstract

The chemical conversion of the top surface of 3-glycidoxypropyldimethylethoxysilane (GPDMES) on hyroxylated silicon surface has been studied as a function of reaction time. A multiple-step procedure was applied in this study. At first, GPDMES molecules were self-assembled on the hydroxylated silicon surface. The second step was the modification of epoxy groups with 3,3'-iminodipropionitrile and the last step was the amidoximation reaction of nitrile groups. Existence of the monolayers covalently attached to silicon surfaces were revealed by X-ray photoelectron spectroscopy and Fourier transform infrared spectroscopy (FT-IR). Modification, conversion and thickness of surfaces were followed by FT-IR and ellipsometry analysis. (C) 2012 Elsevier B.V. All rights reserved.

Source

SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY

Volume

99

URI

https://dx.doi.org/10.1016/j.saa.2012.08.090
https://hdl.handle.net/20.500.12450/1533

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  • WoS İndeksli Yayınlar Koleksiyonu [2182]



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